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Synthesis and Characterisation of a Biolubricant from Cameroon Palm Kernel Seed Oil Using a Locally Produced Base Catalyst from Plantain Peelings

机译:用车前草去皮本地生产的基础催化剂合成喀麦隆棕榈仁籽油中的生物润滑剂并进行表征

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Biolubricant was synthesized from Cameroon palm kernel oil (PKO) by double transesterification, producing methyl esters in the first stage which were then transesterified with trimethylolpropane (TMP) to give the PKO biolubricant in the presence of a base catalyst obtained from plantain peelings (municipal waste). The yields from both catalysts were significantly similar (48% for the locally produced and 51% for the conventional) showing that the locally produced catalyst could be valorized. The synthesized biolubricant was characterized by measuring its physical and chemical properties. The specific gravity of 1.2, ASTM color of 1.5, cloud point of 0°C, pour point of -9°C, viscosities at 40°C of 509.80 cSt and at 100°C of 30.80 cSt, viscosity index of 120, flash point greater than 210°C and a fire point greater than 220°C were obtained. This synthesized biolubricant was found to be comparable to commercial T-46 petroleum lubricant sample produced industrially from mineral sources. We have therefore used local materials to produce a biolubricant using a cheap base catalyst produced from municipal waste.
机译:通过双重酯交换反应从喀麦隆棕榈仁油(PKO)合成生物润滑剂,在第一阶段产生甲酯,然后在由车前草去皮获得的基础催化剂存在下,将其与三羟甲基丙烷(TMP)酯交换以得到PKO生物润滑剂(市政废物)(市政废物) )。两种催化剂的产率都非常相似(本地生产的产率为48%,常规生产的产率为51%),表明本地生产的催化剂可以得到增值。通过测量其物理和化学性质来表征合成的生物润滑剂。比重为1.2,ASTM颜色为1.5,浊点为0°C,倾点为-9°C,40°C时的粘度为509.80 cSt和100°C时的粘度为30.80 cSt,粘度指数为120,闪点获得大于210℃的温度和大于220℃的燃烧点。发现该合成的生物润滑剂与工业上由矿物来源生产的商业T-46石油润滑剂样品具有可比性。因此,我们已经使用本地材料来生产生物润滑剂,而这些廉价的碱催化剂是由城市垃圾产生的。

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