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An Autoclave Effect on the Powder of Poly Methylmethacrylate

机译:高压灭菌对聚甲基丙烯酸甲酯粉末的影响

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Background: Although most of the physical and mechanical properties of denture base resin polymerized by the conventional heat polymerization have been studied, the effect of autoclave processing on these properties has not been fully determined. The effect of autoclave on acrylic powder has not studied before. Materials and methods: Vertex was the heat – cured acrylic denture base material included in this study. A total of 90 specimens were prepared, the specimens were grouped into three control groups of Vertex acrylic resin which(group A) as curing by conventional water- bath technique (74oC for 90 minutes, then boil for 30 minutes, (group B) which curing by water- bath (100°C for 30 minutes), and (group C)which curing by autoclave (120 °C under 1.4 bar for 45 minutes). The other three groups of Vertex acrylic resin after treatment of powder by autoclave in 132 °C for 4 hours, and then grouped into (A1,B1 andC1) which curing as previously. To study the effect of treatment of powder of acrylic resin byautoclave and the effect of autoclave processing. Three tests were conducted surface roughness (profilometer tester), transverse strength (Instron universal testing machine), and surface hardness (Shore D). The results were analyzed to Descriptive Statistics and ANOVA test. Results: There were no significant differences in surface roughness in all studying groups. There was a highly significant difference in transverse strength test results between studying groups. There was a significant difference in surface hardness test results between studying groups. Conclusions: The treatment of powder of acrylic resin by autoclave had no significant differences in surface roughness, but had a highly significant Difference in transverse strength in all test results, and a significant difference in hardness surface test in group B1. The autoclave processing technique might also be a good alternative to the conventional water- bath processing technique.
机译:背景:尽管已研究了通过常规热聚合聚合而成的义齿基体树脂的大多数物理和机械性能,但高压釜处理对这些性能的影响尚未完全确定。高压釜对丙烯酸粉末的作用尚未研究。材料和方法:顶点是本研究中包括的热固化丙烯酸义齿基托材料。总共准备了90个样品,将样品分为三个对照组,分别为Vertex丙烯酸树脂(A组),采用常规水浴技术固化(74oC加热90分钟,然后煮沸30分钟,B组)。水浴(100°C 30分钟)固化,(C组)高压釜(120°C在1.4 bar下45分钟固化),其余三组Vertex丙烯酸树脂经高压釜处理后固化。在132°C下放置4小时,然后分组为如前所述固化的(A1,B1和C1),以研究用高压釜处理丙烯酸树脂粉末的效果和高压釜处理的效果,进行了三个表面粗糙度测试(轮廓仪测试仪) ),横向强度(Instron万能试验机)和表面硬度(邵尔D),将结果进行描述性统计和ANOVA测试分析。结果:在所有研究组中,表面粗糙度均无显着差异,且差异有统计学意义研究组之间横向强度测试结果的差异。研究组之间的表面硬度测试结果存在显着差异。结论:高压釜处理丙烯酸树脂粉末的表面粗​​糙度没有显着差异,但在所有测试结果中横向强度差异均非常显着,而B1组的硬度表面测试差异显着。高压釜处理技术也可能是传统水浴处理技术的良好替代方案。

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