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In-situ TEM Observation of the Interaction between Dislocations and Particles of Cu-added Ferritic Stainless Steel under High-temperature Straining

机译:高温应变下添加Cu的铁素体不锈钢的位错与颗粒间相互作用的原位TEM观察

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Cu is always present in the matrix when ferritic steels were prepared from ferrous scrap. When the ferritic steels are aged thermally, Cu particles start appearing and dispersing finely and homogeneously, which may result the steels strengthened by dispersion strengthening. In this study, the interactions between Cu particles and dislocations were examined via high-temperature in-situ TEM straining. Cu-added ferritic stainless steel (Fe-18.4%Cr-1.5%Cu) was used in the present study. Specimen was aged at 1073 K for 360 ks. Microstructure of specimen was analyzed by JEM-3200FSK and high-temperature in-situ TEM straining was conducted using JEM-1300NEF. Progressing dislocations in matrix contacted with the Cu particle at right angle. This result implies that there is an attractive interaction between dislocations and the Cu particle. Furthermore, dislocations pass through the particle after contacting it, so that the interaction with dislocations and particles should be explained by Srolovitz mechanism.
机译:用铁废料制备铁素体钢时,基体中始终存在铜。当铁素体钢进行热时效处理时,Cu颗粒开始出现并细小且均匀地分散,这可能导致钢通过分散强化而得到强化。在该研究中,通过高温原位TEM应变检查了Cu颗粒与位错之间的相互作用。本研究中使用了添加了铜的铁素体不锈钢(Fe-18.4%Cr-1.5%Cu)。标本在1073 K下老化了360 ks。用JEM-3200FSK分析试样的显微组织,并用JEM-1300NEF进行高温原位TEM应变。与铜粒子成直角接触的基质中的进行性位错。该结果表明,位错与Cu粒子之间存在有吸引力的相互作用。此外,位错与粒子接触后会穿过粒子,因此应通过Srolovitz机理解释与位错和粒子的相互作用。

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