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A novel and compact nanoindentation device for in situ nanoindentation tests inside the scanning electron microscope

机译:用于扫描电子显微镜内部原位纳米压痕测试的新型紧凑型纳米压痕装置

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In situ nanomechanical tests provide a unique insight into mechanical behaviors of materials, such as fracture onset and crack propagation, shear band formation and so on. This paper presents a novel in situ nanoindentationdevice with dimensions of 103mm×74mm×60mm. Integrating the stepper motor, the piezoelectric actuator and the flexure hinge, the device can realize coarse adjustment of the specimen and precision loading and unloading of the indenter automatically. A novel indenter holder was designed to guarantee that the indenter penetrates into and withdraws from the specimen surface vertically. Closed-loop control of the indentation process was established to solve the problem of nonlinearity of the piezoelectric actuator and to enrich the loading modes. The in situ indentation test of Indium Phosphide(InP) inside the scanning electron microscope(SEM) was carried out and the experimental result indicates the feasibility of the developed device.
机译:原位纳米力学测试提供了对材料力学行为的独特见解,例如断裂开始和裂纹扩展,剪切带形成等。本文提出了一种尺寸为103mm×74mm×60mm的新型原位纳米压痕装置。该装置集成了步进电机,压电致动器和挠性铰链,可自动进行标本的粗调和压头的精确装卸。设计了一种新型压头支架,以确保压头垂直穿透并从样品表面退出。建立压痕过程的闭环控制,以解决压电致动器的非线性问题并丰富加载模式。进行了扫描电子显微镜(SEM)内部磷化铟(InP)的原位压痕试验,实验结果表明了该装置的可行性。

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