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The influence of curing times and light curing methods on the polymerization shrinkage stress of a shrinkage-optimized composite with hybrid-type prepolymer fillers

机译:固化时间和光固化方法对混合型预聚物填料的收缩优化复合材料聚合收缩应力的影响

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Objectives. The aim of the study was to determine the influence of different light curing units (LCU) and regimes on the polymerization shrinkage stress (PSS) and the mechanical properties of a nano-hybrid composite. Material and methods. The polymerization shrinkage force (PSF) was measured continuously with compliance compensation for 300 s after photo-initiating the composite, Tetric Evo-Ceram (Ivoclar Vivadent, Schaan, FL, Shade A3) in a Stress-Strain Analyser. Astralis 10, Bluephase and MiniL.E.D LCU with exposure times 10,20 and 40 s were used (C-factor = 0.33, n = 8 per group). Immediately after the PSF measurements, mechanical properties of the samples were measured at the top and the bottom using a Fischerscope H100C (Helmut Fischer GmbH, Sindelfingen, Germany). Statistical analyses were done using one-way ANOVA (p < 0.05) and Tukey post hoc test. Results. Significant differences in the PSS for 10, 20 and 40s polymerization using Astralis 10 were found. The MiniL.E.D recorded low stress values. Modulus of elasticity is high after curing the composite with Astralis 10 at 10, 20 and 40s and for Bluephase 40s. Low moduli of elasticity were recorded for the MiniL.E.D and for the Bluephase 20 and 10 s. The hardness values (HV) followed the same pattern as the modulus of elasticity. The Ramping mode of the MiniL.E.D had prolonged gel point. Conclusions. High intensity LCU produce not just high HV but also high shrinkage, making it important to balance both the effects by choosing the appropriate curing time. Soft-start regimes have no paramount benefit in a LED regarding stresses in the clinical situation.
机译:目标。这项研究的目的是确定不同的光固化单元(LCU)和体系对聚合收缩应力(PSS)和纳米混合复合材料力学性能的影响。材料与方法。在应力应变分析仪中光引发复合材料Tetric Evo-Ceram(Ivoclar Vivadent,Schaan,FL,Shade A3)后,在300 s内用顺应性补偿连续测量聚合收缩力(PSF)。使用暴露时间分别为10,20和40 s的Astralis 10,Bluephase和MiniL.E.D LCU(C因子= 0.33,每组n = 8)。在PSF测量之后,立即使用Fischerscope H100C(Helmut Fischer GmbH,辛德尔芬根,德国)在顶部和底部测量样品的机械性能。使用单向方差分析(p <0.05)和Tukey事后检验进行统计分析。结果。发现使用Astralis 10进行10s,20s和40s聚合时PSS的显着差异。 MiniL.E.D记录到较低的应力值。用Astralis 10在10、20和40s下固化复合材料并在Bluephase 40s下固化后,弹性模量很高。 MiniL.E.D和Bluephase 20和10 s记录到较低的弹性模量。硬度值(HV)遵循与弹性模量相同的模式。 MiniL.E.D的斜坡模式具有延长的胶凝点。结论。高强度LCU不仅产生高HV,而且产生高收缩率,因此通过选择适当的固化时间来平衡两种效果非常重要。就临床情况中的压力而言,软启动方案在LED中没有最重要的好处。

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