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Effect of heat curing treatment on the drying shrinkage behavior and microstructure characteristics of mortar incorporating different content ground granulated blast-furnace slag

机译:热处理对掺入不同含量粒状高炉矿渣的砂浆的干缩性能和微观结构特征的影响

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The effect of heat curing treatment that samples cured from room temperature to an elevated temperature of 60 degrees C for 24 h on the mass loss, drying shrinkage and microstructure of mortar incorporating ground granulated blast-furnace slag (GGBS) as cement replacement at 0%, 20%, 40% and 60% by weight was experimentally investigated in this study. The results show that the heat-treated mortar exhibits lower mass loss compared to the untreated mortar. In addition, when the content of GGBS is 0% or 20%, the heat-treated mortar has a lower drying shrinkage than that of untreated mortar. However, when the content of GGBS is 40% or 60%, the result is the opposite. Moreover, for the heat-treated and untreated mortar, there is an optimal replacement content of about 40% GGBS to restrain drying shrinkage. For the mortar incorporating 0% or 20% GGBS, infrared spectrum (IR) and nuclear magnetic resonance (NMR) analysis reveal that the heat curing treatment mainly leads to a higher degree of silicon polymerization in C-S-H gel and consequently affects the drying shrinkage. For the mortar incorporating 40% or 60% GGBS, scanning electron microscopy (SEM), chemical bound water and mercury intrusion porosimetry (MIP) analysis show that heat curing treatment mainly increases the amount of C-S-H gel and mesopore (50 nm) of mortar and consequently affects the drying shrinkage. (C) 2018 Elsevier Ltd. All rights reserved.
机译:从0到60%从室温到60°C的高温下固化的样品进行的热固化处理对砂浆的质量损失,干燥收缩率和微观结构的影响,砂浆中加入了颗粒状高炉矿渣(GGBS)作为水泥替代品在这项研究中,对20%,40%和60%的重量进行了实验研究。结果表明,与未处理的砂浆相比,热处理的砂浆表现出较低的质量损失。另外,当GGBS的含量为0%或20%时,与未处理的砂浆相比,热处理的砂浆的干燥收缩率更低。但是,当GGBS的含量为40%或60%时,结果相反。此外,对于热处理和未处理的砂浆,GGBS的最佳替代含量约为40%,以抑制干燥收缩。对于掺有0%或20%GGBS的砂浆,红外光谱(IR)和核磁共振(NMR)分析表明,热固化处理主要导致C-S-H凝胶中硅的聚合度更高,从而影响干燥收缩率。对于掺有40%或60%GGBS的砂浆,扫描电子显微镜(SEM),化学结合水和压汞法(MIP)分析表明,热固化处理主要增加砂浆的CSH凝胶和中孔(<50 nm)的量因此影响干燥收缩率。 (C)2018 Elsevier Ltd.保留所有权利。

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