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Photo-Thermoelectric Technique for Anisotropic Thermal Diffusivity Measurements

机译:各向异性热扩散率测量的光热电技术

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摘要

A photo-thermoelectric technique was employed to perform anisotropic thermal diffusivity measurements in nanocomposites and multilayer structures. In this technique a thermal wave is produced into the specimen by absorption of modulated laser radiation while the thermal wave is detected using a fast thermoelectric effect at the junction between a sharp wire probe and the sample surface. To allow effective heating and signal detection, additional thin-film layers may need to be deposited onto the samples. However, heat transport through the layers and into the thermoelectric probe may affect the thermal transport measurements. This work presents a heat conduction model that takes these effects into account and can be used to guide the selection of the probe and thin-film materials and thicknesses such that the accuracy of the thermal measurements is minimally affected. The discussion of the experimental technique is illustrated with simulation results, calibration experiments, and an example of anisotropic thermal diffusivity characterization in aligned multiwall carbon nanotube arrays.
机译:使用光热电技术在纳米复合材料和多层结构中执行各向异性热扩散率测量。在该技术中,通过吸收调制的激光辐射将热波产生到样本中,同时在尖锐的线探针和样品表面之间的接合处使用快速热电效应检测热波。为了有效加热和检测信号,可能需要在样品上沉积其他薄膜层。但是,通过层进入热电探针的热传输可能会影响热传输测量。这项工作提出了一种考虑了这些影响的热传导模型,可用于指导探针,薄膜材料和厚度的选择,从而使对热测量精度的影响降至最低。通过模拟结果,校准实验以及对准的多壁碳纳米管阵列中各向异性热扩散特性的例子说明了对实验技术的讨论。

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