Water-controlled synthesis and single-crystal structural transformations of a cyanide-bridged W(Ⅳ)-Ni(Ⅱ) molecular wheel complex and 3D networks

Dao-Peng Zhang; Li-Fang Zhang; Guo-Ling Li; Zhong-Hai Ni

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Water-controlled synthesis and single-crystal structural transformations of a cyanide-bridged W(Ⅳ)-Ni(Ⅱ) molecular wheel complex and 3D networks

机译：氰化物桥联的W（Ⅳ）-Ni（Ⅱ）分子轮络合物和3D网络的水控合成和单晶结构转变

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摘要

One cyanide-bridged W(Ⅳ)-Ni(Ⅱ) wheel-like complex and two three-dimensional (3D) networks can be directly synthesized based on K_4[W(CN)_8] and [Ni(L)](ClO_4)_2 precursors by controlling the quantity of water in organic solvent. The water-controlled single-crystal structural transformations among these complexes are described.

机译：基于K_4 [W（CN）_8]和[Ni（L）]（ClO_4）可以直接合成一个氰化物桥联的W（Ⅳ）-Ni（Ⅱ）轮状络合物和两个三维（3D）网络。通过控制有机溶剂中的水量来添加_2个前体。描述了这些配合物中水控制的单晶结构转变。

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《Chemical Communications》 |2013年第83期|9582-9584|共3页
作者
Dao-Peng Zhang; Li-Fang Zhang; Guo-Ling Li; Zhong-Hai Ni;
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School of Chemical Engineering and Technology, China University of Mining and Technology, XuZhou 221116, P. R. China,College of Chemical Engineering, Shandong University of Technology, Zibo 255049, P. R. China,Department of Chemistry, University of Science and Technology Beijing, Beijing 100083, P. R. China;

School of Chemical Engineering and Technology, China University of Mining and Technology, XuZhou 221116, P. R. China;

School of Chemical Engineering and Technology, China University of Mining and Technology, XuZhou 221116, P. R. China;

School of Chemical Engineering and Technology, China University of Mining and Technology, XuZhou 221116, P. R. China;

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Water-controlled synthesis and single-crystal structural transformations of a cyanide-bridged W(Ⅳ)-Ni(Ⅱ) molecular wheel complex and 3D networks

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