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Hierarchical Nickel nanowire synthesis using polysorbate 80 as capping agent

机译:聚山梨酯80为封端剂的镍纳米线的分层合成

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Nanomaterials find applications in multiple fields including food and beverages, waste water management, electrical and electronics due to their interesting properties. These properties can be fine-tuned using various synthesis techniques ranging from solid state route to different wet chemical techniques like precipitation, sol-gel, hydrothermal and solvothermal methods Here, we report a simple wet chemical synthesis of nickel nanoparticles using Tween 80 as the capping agent. Scanning electron microscopy (SEM) revealed a hierarchical nanowire- like morphology with thorn like sharp edges while the presence of nickel in the sample was confirmed by energy dispersive spectroscopy (EDS). X-ray diffraction studies ascertained the crystalline nature of nickel nanowires and also the purity of the as-synthesized nanowires. Transmission electron Microscopy (TEM) and Selected Area Electron Diffraction (SAED) analysis of the sample indicated the existence of a small quantity of nickel hydroxide. The magnetic property of the synthesized nickel samples studied using vibrating sample magnetometer (VSM) revealed a high saturation magnetization of similar to 43 emug(-1). Antibacterial activity studies confirmed that nickel nanowire exhibited an excellent bactericidal activity against both gram-positive and gram-negative bacteria which could be attributed to the morphology of the nickel nanowires. (C) 2017 Elsevier B.V. All rights reserved.
机译:纳米材料因其有趣的特性而在多个领域得到了应用,包括食品和饮料,废水管理,电气和电子。可以使用各种合成技术对这些特性进行微调,这些合成技术从固态途径到不同的湿化学技术,例如沉淀法,溶胶-凝胶法,水热法和溶剂热法,在这里,我们报告了使用Tween 80作为封端的镍纳米粒子的简单湿法化学合成代理商。扫描电子显微镜(SEM)显示出具有刺状尖锐边缘的分层的纳米线状形态,而样品中镍的存在则通过能量色散光谱法(EDS)得以证实。 X射线衍射研究确定了镍纳米线的晶体性质以及合成后的纳米线的纯度。样品的透射电子显微镜(TEM)和选择区域电子衍射(SAED)分析表明存在少量的氢氧化镍。使用振动样品磁力计(VSM)研究的合成镍样品的磁性能显示出高饱和磁化强度,类似于43 emug(-1)。抗菌活性研究证实,镍纳米线对革兰氏阳性和革兰氏阴性细菌均表现出优异的杀菌活性,这可归因于镍纳米线的形态。 (C)2017 Elsevier B.V.保留所有权利。

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