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Fabrication of SnO2 Composite Nanofiber-Based Gas Sensor Using the Electrospinning Method for Tetrahydrocannabinol (THC) Detection

机译:使用静电纺丝法检测四氢大麻酚(THC)的SnO2复合纳米纤维基气体传感器的制备

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摘要

This paper presents the development of a metal oxide semiconductor (MOS) sensor for the detection of volatile organic compounds (VOCs) which are of great importance in many applications involving either control of hazardous chemicals or noninvasive diagnosis. In this study, the sensor is fabricated based on tin dioxide (SnO ) and poly(ethylene oxide) (PEO) using electrospinning. The sensitivity of the proposed sensor is further improved by calcination and gold doping. The gold doping of composite nanofibers is achieved using sputtering, and the calcination is performed using a high-temperature oven. The performance of the sensor with different doping thicknesses and different calcination temperatures is investigated to identify the optimum fabrication parameters resulting in high sensitivity. The optimum calcination temperature and duration are found to be 350 °C and 4 h, respectively and the optimum thickness of the gold dopant is found to be 10 nm. The sensor with the optimum fabrication process is then embedded in a microchannel coated with several metallic and polymeric layers. The performance of the sensor is compared with that of a commercial sensor. The comparison is performed for methanol and a mixture of methanol and tetrahydrocannabinol (THC) which is the primary psychoactive constituent of cannabis. It is shown that the proposed sensor outperforms the commercial sensor when it is embedded inside the channel.
机译:本文介绍了一种用于检测挥发性有机化合物(VOC)的金属氧化物半导体(MOS)传感器的开发,该传感器在涉及危险化学品控制或非侵入性诊断的许多应用中具有重要意义。在这项研究中,传感器是通过静电纺丝法基于二氧化锡(SnO)和聚环氧乙烷(PEO)制成的。通过煅烧和金掺杂进一步提高了所提出的传感器的灵敏度。使用溅射实现复合纳米纤维的金掺杂,并使用高温烘箱进行煅烧。研究了具有不同掺杂厚度和不同煅烧温度的传感器的性能,以确定导致高灵敏度的最佳制造参数。发现最佳煅烧温度和持续时间分别为350℃和4h,并且发现金掺杂剂的最佳厚度为10nm。然后将具有最佳制造工艺的传感器嵌入到覆盖有多个金属和聚合物层的微通道中。将传感器的性能与商用传感器的性能进行比较。对甲醇以及作为大麻主要精神活性成分的甲醇与四氢大麻酚(THC)的混合物进行了比较。结果表明,所建议的传感器嵌入到通道中后,性能优于商用传感器。

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