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Effect of Thermocycling Surface Treatments and Microstructure on the Optical Properties and Roughness of CAD-CAM and Heat-Pressed Glass Ceramics

机译:热循环表面处理和微结构对CAD-CAM和热压玻璃陶瓷的光学性能和粗糙度的影响

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摘要

Dental ceramic restorations are widely spread nowadays due to their aesthetics and biocompatibility. In time, the colour and structure of these ceramic materials can be altered by aging processes. How does artificial aging affect the optical and surface roughness of ceramics? This study aims to assess the effect of thermocycling, surface treatments and microstructure upon translucency, opalescence and surface roughness on CAD-CAM and heat-pressed glass-ceramic. Forty-eight samples (1.5 mm thickness) were fabricated from six types of A2 MT ceramic: heat-pressed and milled glass-ceramic (feldspathic, lithium disilicate and zirconia reinforced lithium silicate). The samples were obtained respecting the manufacturer’s instructions. The resulted surfaces (n = 96) were half glazed and half polished. The samples were subjected to thermocycling (10,000 cycles) and roughness values (Ra and Rz), colour coordinates (L*, a*, b*) and microstructural analyses were assessed before and after thermocycling. Translucency (TP) and opalescence (OP) were calculated. Values were statistically analysed using ANOVA test (one way). TP and OP values were significantly different between heat-pressed and milled ceramics before and also after thermocycling ( < 0.001). Surface treatments (glazing and polishing) had a significant effect on TP and OP and surface roughness ( < 0.05). The heat-pressed and milled zirconia reinforced lithium silicate glass-ceramic experienced a loss in TP and OP. Ra and Rz increased for the glazed samples, TP and OP decreased for all the samples after thermocycling. Microstructural analyse revealed that glazed surfaces were more affected by the thermocycling and especially for the zirconia reinforced lithium silicate ceramic. Optical properties and surface roughness of the chosen ceramic materials were affected by thermocycling, surface treatments and microstructural differences. The least affected of the ceramics was the lithium disilicate ceramic heat-pressed polished and glazed.
机译:牙科陶瓷修复体由于其美学和生物相容性,如今已广泛传播。随着时间的流逝,这些陶瓷材料的颜色和结构会因时效过程而改变。人工时效如何影响陶瓷的光学和表面粗糙度?这项研究旨在评估热循环,表面处理和微结构对CAD-CAM和热压玻璃陶瓷的半透明,乳光和表面粗糙度的影响。用六种类型的A2 MT陶瓷制成四十八个样品(厚度为1.5 mm):热压和磨碎的玻璃陶瓷(长石,二硅酸锂和氧化锆增强硅酸锂)。按照制造商的说明获得样品。将得到的表面(n = 96)进行半釉和半抛光。对样品进行热循环(10,000个循环),并在热循环之前和之后评估粗糙度值(Ra和Rz),色坐标(L *,a *,b *)和微观结构分析。计算半透明性(TP)和乳光性(OP)。使用方差分析检验(单向)对值进行统计分析。热压和研磨后的陶瓷在热循环之前和之后的TP和OP值显着不同(<0.001)。表面处理(上光和抛光)对TP和OP以及表面粗糙度有显着影响(<0.05)。热压和研磨的氧化锆增强硅酸锂玻璃陶瓷的TP和OP降低。玻璃样品的Ra和Rz增加,热循环后所有样品的TP和OP降低。微观结构分析表明,釉面受热循环的影响更大,尤其是对于氧化锆增强的硅酸锂陶瓷而言。所选陶瓷材料的光学性能和表面粗糙度受热循环,表面处理和微观结构差异的影响。对陶瓷影响最小的是热压抛光和上釉的二硅酸锂陶瓷。

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