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Synthesis and Tribological Properties of WSe2Nanorods

机译:WSe2纳米棒的合成及其摩擦学性能

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摘要

The WSe2nanorods were synthesized via solid-state reaction method and characterized by X-ray diffractometer, TEM, and HRTEM. The results indicated the WSe2compounds had rod-like structures with diameters of 10–50 nm and lengths of 100–400 nm, and the growth process of WSe2nanorods was discussed on the basis of the experimental facts. The tribological properties of WSe2nanorods as additives in HVI500 base oil were investigated by UMT-2 multispecimen tribotester. Under the determinate conditions, the friction coefficient of the base oil containing WSe2nanorods was lower than that of the base oil, and decreased with increasing mass fraction of WSe2nanorods when it was <7 wt.%. Moreover, the base oil with the additives was rather suited to high load and high rotating speed. A combination of rolling friction, sliding friction, and stable tribofilm on the rubbing surface could explain the good friction and wear properties of WSe2nanorods as additives.
机译:通过固相反应法合成了WSe2纳米分子,并通过X射线衍射仪,TEM和HRTEM对其进行了表征。结果表明,WSe2化合物具有直径为10–50 nm,长度为100–400 nm的棒状结构,并根据实验事实讨论了WSe2纳米棒的生长过程。通过UMT-2多样品三botester研究了WSe2nanodods在HVI500基础油中作为添加剂的摩擦学性能。在确定的条件下,含WSe2nanorods的基础油的摩擦系数低于基础油,并且当WSe2nanorods的质量分数小于7 wt%时,摩擦系数随WSe2nanorods的质量分数的增加而降低。此外,具有添加剂的基础油相当适合于高负荷和高转速。滚动摩擦,滑动摩擦和稳定的摩擦膜在摩擦表面上的结合可以解释WSe2纳米棒作为添加剂的良好摩擦和磨损性能。

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