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Microstructure and performance of rare earth element-strengthened plasma-facing tungsten material

机译:稀土元素强化等离子面钨材料的组织与性能

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摘要

Pure W and W-(2%, 5%, 10%) Lu alloys were manufactured via mechanical alloying for 20 h and a spark plasma sintering process at 1,873 K for 2 min. The effects of Lu doping on the microstructure and performance of W were investigated using various techniques. For irradiation performance analysis, thermal desorption spectroscopy (TDS) measurements were performed from room temperature to 1,000 K via infrared irradiation with a heating rate of 1 K/s after implantations of He+ and D+ ions. TDS measurements were conducted to investigate D retention behavior. Microhardness was dramatically enhanced, and the density initially increased and then decreased with Lu content. The D retention performance followed the same trend as the density. Second-phase particles identified as Lu2O3 particles were completely distributed over the W grain boundaries and generated an effective grain refinement. Transgranular and intergranular fracture modes were observed on the fracture surface of the sintered W-Lu samples, indicating some improvement of strength and toughness. The amount and distribution of Lu substantially affected the properties of W. Among the investigated alloy compositions, W-5%Lu exhibited the best overall performance.
机译:纯W和W-(2%,5%,10%)Lu合金是通过机械合金化20 h和在1873 K下进行2 min的火花等离子体烧结工艺制造的。使用各种技术研究了Lu掺杂对W的微观结构和性能的影响。为了进行辐射性能分析,在植入He + 和D +后,通过红外辐射以1 K / s的加热速率从室温到1,000 K进行热解吸光谱(TDS)测量。 离子。进行TDS测量以研究D保留行为。显微硬度显着提高,并且密度随Lu含量的增加先增加后降低。 D保留性能遵循与密度相同的趋势。识别为Lu2O3颗粒的第二相颗粒完全分布在W晶界上,并产生了有效的晶粒细化。在烧结的W-Lu样品的断裂表面上观察到了晶间和晶间断裂模式,表明强度和韧性有所改善。 Lu的量和分布基本上影响W的性能。在所研究的合金组成中,W-5%Lu表现出最佳的整体性能。

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