首页> 美国卫生研究院文献>Journal of Synchrotron Radiation >Dynamic adaptive X-ray optics. Part II. High-speed piezoelectric bimorph deformable Kirkpatrick–Baez mirrors for rapid variation of the 2D size and shape of X-ray beams
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Dynamic adaptive X-ray optics. Part II. High-speed piezoelectric bimorph deformable Kirkpatrick–Baez mirrors for rapid variation of the 2D size and shape of X-ray beams

机译:动态自适应X射线光学器件。第二部分高速压电双压电晶片可变形Kirkpatrick-Baez反射镜可快速改变X射线束的二维尺寸和形状

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摘要

The tangential curvature of actively bent X-ray mirrors at synchrotron radiation and X-ray free-electron laser (XFEL) facilities is typically only changed every few hours or even days. This operation can take tens of minutes for active optics with multiple bending actuators and often requires expert guidance using in situ monitoring devices. Hence, the dynamic performance of active X-ray optics for synchrotron beamlines has historically not been exploited. This is in stark contrast to many other scientific fields. However, many areas of synchrotron radiation and XFEL science, including macromolecular crystallography, could greatly benefit from the ability to change the size and shape of the X-ray beam rapidly and continuously. The advantages of this innovative approach are twofold: a large reduction in the dead time required to change the size of the X-ray beam for different-sized samples and the possibility of making multiple changes to the beam during the measurement of a single sample. In the preceding paper [Part I; Alcock, Nistea, Signorato & Sawhney (2019), J. Synchrotron Rad. >26, 36–44], which accompanies this article, high-speed visible-light Fizeau interferometry was used to identify the factors which influence the dynamic bending behaviour of piezoelectric bimorph deformable X-ray mirrors. Building upon this ex situ metrology study, provided here is the first synchrotron radiation beamline implementation of high-speed adaptive X-ray optics using two bimorphs operating as a Kirkpatrick–Baez pair. With optimized substrates, novel opto-mechanical holders and a next-generation high-voltage power supply, the size of an X-ray beam was rapidly and repeatedly switched in <10 s. Of equal importance, it is also shown that compensation of piezoelectric creep ensures that the X-ray beam size remains stable for more than 1 h after making a major change. The era of high-speed adaptive X-ray optics for synchrotron radiation and XFEL beamlines has begun.
机译:在同步加速器辐射和X射线自由电子激光(XFEL)设备处,主动弯曲的X射线镜的切向曲率通常仅每隔几小时甚至几天才改变一次。对于带有多个弯曲致动器的有源光学系统,此操作可能要花费数十分钟,并且经常需要使用现场监控设备进行专家指导。因此,历史上没有开发用于同步加速器光束线的有源X射线光学器件的动态性能。这与许多其他科学领域形成鲜明对比。但是,同步加速器辐射和XFEL科学的许多领域,包括大分子晶体学,都可以从快速连续地改变X射线束的大小和形状的能力中受益匪浅。这种创新方法的优点是双重的:对于不同尺寸的样品,改变X射线束的大小所需的停滞时间大大减少,并且在单个样品的测量过程中对束进行多次更改的可能性。在上一篇论文中[第一部分; Alcock,Nistea,Signorato和Sawhney(2019),J.Synchrotron Rad。 > 26 ,36-44],本文使用高速可见光菲索干涉仪来确定影响压电双压电晶片可变形X射线反射镜动态弯曲行为的因素。在此异地计量学研究的基础上,这里提供了使用两个作为Kirkpatrick-Baez对的双压电晶片对高速自适应X射线光学器件进行同步辐射辐射线的第一个实现。通过优化的基板,新颖的光电机械支架和下一代高压电源,X射线束的大小得以快速重复地切换,时间小于10秒。同样重要的是,还显示出压电蠕变的补偿可确保在进行重大更改后,X射线束的大小在超过1 h的时间内保持稳定。用于同步加速器辐射和XFEL光束线的高速自适应X射线光学器件的时代已经开始。

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