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Analysis of the Chemical Composition of the Essential Oil of Polygonum minus Huds. Using Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GC-TOF MS)

机译:虎杖精油化学成分分析。使用二维气相色谱-飞行时间质谱(GC-TOF MS)

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摘要

The essential oil in leaves of Polygonum minus Huds., a local aromatic plant, were identified by a pipeline of gas chromatography (GC) techniques coupled with mass-spectrometry (MS), flame ionization detector (FID) and two dimensional gas chromatography time of flight mass spectrometry (GC×GC–TOF MS). A total of 48 compounds with a good match and high probability values were identified using this technique. Meanwhile, 42 compounds were successfully identified in this study using GC-MS, a significantly larger number than in previous studies. GC-FID was used in determining the retention indices of chemical components in P. minus essential oil. The result also showed the efficiency and reliability were greatly improved when chemometric methods and retention indices were used in identification and quantification of chemical components in plant essential oil.
机译:通过一系列气相色谱(GC)技术与质谱(MS),火焰电离检测器(FID)和二维气相色谱时间联用,鉴定了本地芳香植物何首乌的叶子中的精油。飞行质谱(GC×GC–TOF MS)。使用该技术,共鉴定出48种具有良好匹配性和高概率值的化合物。同时,使用GC-MS在本研究中成功鉴定出42种化合物,其数量比以前的研究大得多。 GC-FID用于确定假单胞菌精油中化学成分的保留指数。结果还表明,将化学计量方法和保留指数用于植物精油中化学成分的鉴定和定量时,效率和可靠性大大提高。

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