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Determination of the Authenticity of Dairy Products on the Basis of Fatty Acids and Triacylglycerols Content using GC Analysis

机译:气相色谱分析法测定脂肪酸和三酰甘油含量对乳制品真伪的影响

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摘要

Milk fat is an important food component, and plays a significant role in the economics, functional nutrition, and chemical properties of dairy products. Dairy products also contain nutritional resources and essential fatty acids (FAs). Because of the increasing demand for dairy products, milk fat is a common target in economic fraud. Specifically, milk fat is often replaced with cheaper or readily available vegetable oils or animal fats. In this study, a method for the discrimination of milk fat was developed, using FAs profiles, and triacylglycerols (TGs) profiles. A total of 11 samples were evaluated: four milk fats (MK), four vegetable oils (VG), two pork lards (PL), and one beef tallow (BT). Gas chromathgraphy analysis were performed, to monitor the FAs content and TGs composition in MK, VG, PL, and BT. The result showed that qualitative determination of the MK of samples adulterated with different vegetable oils and animal fats was possible by a visual comparision of FAs, using C14:0, C16:0, C18:1n9c, C18:0, and C18:2n6c, and of TGs, using C36, C38, C40, C50, C52, and C54 profiles. Overall, the objective of this study was to evaluate the potential of the use of FAs and TGs in the detection of adulterated milk fat, and accordingly characterize the samples by the adulterant oil source, and level of adulteration. Also, based on this preliminary investigation, the usefulness of this approach could be tested for other oils in the future.
机译:乳脂是重要的食品成分,在乳制品的经济性,功能性营养和化学性质中起着重要作用。乳制品还包含营养资源和必需脂肪酸(FAs)。由于对乳制品的需求不断增加,乳脂成为经济欺诈中的常见目标。具体而言,牛奶脂肪通常被便宜或容易获得的植物油或动物脂肪代替。在这项研究中,使用FAs谱和三酰基甘油(TGs)谱开发了一种鉴别乳脂的方法。总共评估了11个样品:四种牛奶脂肪(MK),四种植物油(VG),两种猪油(PL)和一种牛脂(BT)。进行气相色谱分析,以监测MK,VG,PL和BT中的FA含量和TG组成。结果表明,通过使用C14:0,C16:0,C18:1n9c,C18:0和C18:2n6c对FA进行目测比较,可以对掺有不同植物油和动物脂肪的样品的MK进行定性测定,和TG,使用C36,C38,C40,C50,C52和C54配置文件。总体而言,本研究的目的是评估使用FA和TG来检测掺假乳脂的潜力,并相应地通过掺假油来源和掺假水平来表征样品。同样,基于此初步调查,将来可以在其他油中测试这种方法的有效性。

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