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Effect of Milling Time on the Microstructure Physical and Mechanical Properties of Al-Al2O3 Nanocomposite Synthesized by Ball Milling and Powder Metallurgy

机译:研磨时间对球磨和粉末冶金合成的Al-Al2O3纳米复合材料的微观结构物理力学性能的影响

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摘要

The effect of milling time on the morphology, microstructure, physical and mechanical properties of pure Al-5 wt % Al2O3 (Al-5Al2O3) has been investigated. Al-5Al2O3 nanocomposites were fabricated using ball milling in a powder metallurgy route. The increase in the milling time resulted in the homogenous dispersion of 5 wt % Al2O3 nanoparticles, the reduction of particle clustering, and the reduction of distances between the composite particles. The significant grain refining during milling was revealed which showed as a reduction of particle size resulting from longer milling time. X-Ray diffraction (XRD) analysis of the nanocomposite powders also showed that designated ball milling contributes to the crystalline refining and accumulation of internal stress due to induced severe plastic deformation of the particles. It can be argued that these morphological and microstructural variations of nanocomposite powders induced by designated ball milling time was found to contribute to an improvement in the density, densification, micro-hardness (HV), nano-hardness (HN), and Young’s modulus (E) of Al-5Al2O3 nanocomposites. HV, HN, and E values of nanocomposites were increased by ~48%, 46%, and 40%, after 12 h of milling, respectively.
机译:研究了研磨时间对纯Al-5 wt%Al2O3(Al-5Al2O3)的形态,微观结构,物理和机械性能的影响。 Al-5Al2O3纳米复合材料是通过球磨在粉末冶金工艺中制备的。研磨时间的增加导致5 wt%Al2O3纳米颗粒的均匀分散,颗粒簇的减少以及复合颗粒之间距离的减少。显示出在研磨过程中显着的晶粒细化,这表明由于更长的研磨时间而导致粒度减小。纳米复合材料粉末的X射线衍射(XRD)分析还表明,指定的球磨由于颗粒的严重塑性变形,有助于晶体的细化和内应力的积累。可以说,发现由指定的球磨时间引起的纳米复合粉末的这些形态和微观结构变化有助于提高密度,致密化,微硬度(HV),纳米硬度(HN)和杨氏模量( E)Al-5Al2O3纳米复合材料。研磨12小时后,纳米复合材料的HV,HN和E值分别增加了〜48%,46%和40%。

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