4,4-二过氧化叔丁基-1-羟基环已烷引发剂的合成研究

摘要

利用缩醛反应合成了可作为引发剂的化合物4,4-二过氧化叔丁基-1-羟基环已烷,并通过元素分析、1H NMR和FTIR等方法分析鉴定了其化学结构,证明了该化合物被成功合成.同时探讨了不同温度下的合成产率,确定了其最佳反应温度是10℃,产率为86.2%.%The compound 4,4-bis-tert-butylperoxy cyclohexanol which can be used as an initiator was synthesized by acetalization reaction.The chemical structure of the compound was confirmed by elemental analysis,1H NMR and FTIR.At the same time the optimal reaction temperature was 10 ℃ and the yield was 86.2%.