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Creep and mechanical behavior of silicon nitride whisker-reinforced silicon nitride composite ceramics.

机译:氮化硅晶须增强的氮化硅复合陶瓷的蠕变和力学性能。

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摘要

Monolithic {dollar}rm Sisb3Nsb4{dollar} ceramics, hot-pressed with either 3% MgO or 6% {dollar}rm Ysb2Osb3{dollar} additives and their respective composites, with additions of 5% and 10% {dollar}rm Sisb3Nsb4{dollar} whiskers, were creep tested at 1250, 1300 and 1350{dollar}spcirc{dollar}C with stresses varying from 40 to 90 MPa. A new creep flexure test, the "dynamic beam profile method", capable of measuring both load-point and center-of-the-beam displacements, was developed. This configuration permitted in-situ profiling of the beam throughout the test, so that the compressive and tensile deformations in the outer fibers, together with neutral axis displacement, could be determined in real time. Analysis of the curvature of the beam was combined with the closed form solution proposed by Chen and Chuang (1990), and a modification of their analysis developed in this research, to obtain creep exponents from the tensile and compressive outer fibers. These exponents were identical to those determined from tensile and compressive creep tests, and the evolution of creep damage in the tensile outer fibers of the creep flexure tests was also identical to that observed in tensile creep tests at the same temperature.; The {dollar}rm Sisb3Nsb4{dollar} whisker reinforcement was found neither to improve the creep rates nor the creep lives compared to the monolithic material. The reliability of the materials was not improved by the addition of whiskers, but depended on the cleanliness of the material. At 1250{dollar}spcirc{dollar}C deformation resulted in the growth of facet-sized cavities. At 1300{dollar}spcirc{dollar}C the facet-sized cavities linked to form microcracks, and at 1350{dollar}spcirc{dollar}C the microcracks linked to form macrocracks. The creep exponents associated with these deformation mechanisms ranged between three and five. The results showed that the new dynamic beam profile method was capable of analyzing both the tensile and compressive creep behavior of ceramic and ceramic composite materials.
机译:用3%MgO或6%{rm} rm Ysb2Osb3 {dollar}添加剂及其各自的复合材料,以及5%和10%{rmal} rm Sisb3Nsb4 {美元晶须在1250、1300和1350 {spcirc {dollar} C}下进行了蠕变测试,应力范围为40到90 MPa。开发了一种新的蠕变挠曲测试,即“动态光束轮廓法”,它能够测量载荷点和梁的中心位移。这种配置允许在整个测试过程中对光束进行原位剖析,从而可以实时确定外部纤维中的压缩变形和拉伸变形以及中性轴位移。梁的曲率分析与Chen和Chuang(1990)提出的封闭形式解决方案相结合,并对本研究中对它们​​的分析进行了修改,从而从拉伸和压缩外纤维中获得了蠕变指数。这些指数与从拉伸和压缩蠕变试验确定的指数相同,蠕变挠曲试验的拉伸外纤维中蠕变损伤的演变也与在相同温度下的拉伸蠕变试验中观察到的相同。发现与单块材料相比,{rm} Sisb3Nsb4 {dollar}晶须增强材料不会提高蠕变速率或蠕变寿命。添加晶须并不能提高材料的可靠性,而是取决于材料的清洁度。在1250 {sp} {dol} C时,变形导致刻面大小的孔洞增大。在1300℃时,小面尺寸的空腔连接形成微裂纹,而在1350℃时,微裂纹连接形成宏观裂纹。与这些变形机制相关的蠕变指数在三到五之间。结果表明,新的动态光束轮廓法能够分析陶瓷和陶瓷复合材料的拉伸和压缩蠕变行为。

著录项

  • 作者单位

    Illinois Institute of Technology.;

  • 授予单位 Illinois Institute of Technology.;
  • 学科 Engineering Materials Science.; Engineering Metallurgy.
  • 学位 Ph.D.
  • 年度 1996
  • 页码 287 p.
  • 总页数 287
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 工程材料学;冶金工业;
  • 关键词

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