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Effects of deformation on annealing and precipitation behavior of aluminum alloys.

机译:变形对铝合金退火和析出行为的影响。

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摘要

Several commercial aluminum alloys were used to study the effects of deformation on their annealing and precipitation behavior. The alloys were solution heat treated and quenched. Deformation was made by rolling at room temperature with reductions from 0% to 90%. Annealing was subsequent to cold rolling, annealing temperatures from 100{dollar}spcirc{dollar}C to 400{dollar}spcirc{dollar}C and annealing times from 0.5 hour to 24 hours. Conductivity and microhardness were used to measure the changes of properties after cold rolling and annealing. Microstructural evolution was carried out by using optical microscopy (OM) and transmission electron microscopy (TEM).; The supersaturated heat-treatable (precipitation hardening) Al-4wt% Cu, 2024, 6061 and 7475 aluminum alloys had hardening rates higher than those of non-heat-treatable aluminum alloys. As previously reported the strain hardening of aluminum alloys was increased by high solute levels. The increased microhardness {dollar}Delta{dollar}H was found to be described by {dollar}Delta{dollar}H = K{dollar}varepsilonsp{lcub}rm n{rcub}{dollar}, and K increased as the solute increased. On low temperature annealing, there was little loss of strain hardening by recovery until the electrical conductivity rose, indicating precipitation. Measurement of decreasing electrical conductivity and rapid strain hardening, especially in 7475 aluminum alloys, appears to indicate that GP zones formed during cold rolling. The conductivity of naturally aged 7475 aluminum alloys decreased after cold rolling--indicating that the GP zones are essentially stable during deformation.; After applying high reduction ({dollar}ge{dollar}60%) of cold-rolling prior to aging, no significant precipitation hardening was found on aging the 4 heat-treatable aluminum alloys. From TEM observation, round-shaped precipitates were found in alloys with 90% reduction and rod or plate-shaped precipitates were found in undeformed alloys.; By using OM and TEM, it is confirmed that true recrystallization did not occur in heat-treatable Al-4wt% Cu, 2024, 6061 and 7475 aluminum alloys when annealing temperatures are below the solvus temperature. The subgrains appear to coarsen by extended recovery.
机译:几种商用铝合金用于研究变形对其退火和析出行为的影响。将合金固溶热处理并淬火。通过在室温下从0%减少到90%轧制来进行变形。退火是在冷轧之后进行的,退火温度从100 {spC到400℃,退火时间从0.5小时到24小时。电导率和显微硬度用于测量冷轧和退火后的性能变化。通过使用光学显微镜(OM)和透射电子显微镜(TEM)进行微观结构演变。 Al-4wt%Cu,2024、6061和7475铝合金过饱和可热处理(沉淀硬化)铝合金的硬化速率高于不可热处理的铝合金。如先前报道的那样,铝合金的应变硬化由于高溶质水平而增加。发现增加的显微硬度{dollar} Delta {dollar} H由{dollar} Delta {dollar} H = K {dollar} varepsilonsp {lcub} rm n {rcub} {dollar}来描述,并且K随着溶质的增加而增加。在低温退火下,直到恢复到电导率上升为止几乎没有因恢复而引起的应变硬化损失,这表明沉淀。测量导电性下降和快速应变硬化,尤其是在7475铝合金中,似乎表明在冷轧过程中形成了GP区。自然时效的7475铝合金的电导率在冷轧后降低-表明GP区在变形过程中基本稳定。在进行时效处理之前,先进行大量的冷轧轧制({dollar} ge {dollar} $ 60%),但在这4种可热处理铝合金的时效处理中未发现明显的沉淀硬化。从透射电镜观察,还原率降低90%的合金中发现了圆形沉淀,未变形合金中发现了棒状或板状沉淀。通过使用OM和TEM,证实了当退火温度低于固溶温度时,可热处理的Al-4wt%Cu,2024、6061和7475铝合金中不会发生真正的重结晶。延长恢复后,亚颗粒似乎会变粗。

著录项

  • 作者

    Wu, Kun-Fong.;

  • 作者单位

    Drexel University.;

  • 授予单位 Drexel University.;
  • 学科 Engineering Metallurgy.
  • 学位 Ph.D.
  • 年度 1997
  • 页码 292 p.
  • 总页数 292
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 冶金工业;
  • 关键词

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