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The use of supercritical fluid extraction for the treatment of oil contaminated drilling waste.

机译:超临界流体萃取技术用于处理石油污染的钻井废料。

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Supercritical fluid extraction (SFE) with CO2 is a promising new technique to treat drilling waste. In this research, two types of drilling waste were investigated: centrifuge underflow cuttings and invert cuttings. The extraction conditions studied were from 8.96 MPa to 15.2 MPa for pressure and from 40°C to 60°C for temperature.; Within the conditions tested, the suggested operating conditions were 14.5 MPa and 40°C. Under these conditions, the treated cuttings appeared dry, powder-like, and light in color. The high extraction efficiencies indicated that the SFE process was able to reduce the oil content from 19.4% to approximately 0.3%, which is below regulatory guidelines.; Good mixing by a ribbon blender led to high extraction efficiencies. The use of high water contents (1:1 drilling wastewater ratio) and drying agents did not affect the extraction efficiency.; The results are helpful to determine the loading ratio of cuttings in SC CO2 at larger scales.
机译:含二氧化碳的超临界流体萃取(SFE)是一种有前途的处理钻探废料的新技术。在这项研究中,研究了两种类型的钻井废料:离心机下溢屑和倒置屑。研究的萃取条件为压力为8.96 MPa至15.2 MPa,温度为40°C至60°C。在测试条件下,建议的工作条件为14.5 MPa和40°C。在这些条件下,处理后的切屑显得干燥,呈粉末状且颜色浅。较高的萃取效率表明SFE工艺能够将油含量从19.4%降低至约0.3%,这低于监管准则。螺带式搅拌机的良好混合可提高提取效率。高水含量(钻井废水比例为1:1)和干燥剂的使用不会影响萃取效率。这些结果有助于确定SC CO2中钻屑的较大比例。

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