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Crystal microstructure of PbTe/Si and PbTe/SiO_2/Si thin films

机译:PbTe / Si和PbTe / SiO_2 / Si薄膜的晶体微观结构

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A modified 'hot wall' technique (HWE) is used for growth of PbTe thin films directly on Si(100) high ohmic substrates both with and without any buffer layers. The previously formed SiO_2 films have been used as buffer layers. The crystal microstructure of PbTe thin films has been studied by an etching pits method, SEM, RHEED and by X-ray analysis which is able to determine the X-ray rocking curve profiles and line width with high precision.. It has been found that these PbTe/Si and PbTe/SiO_2/Si thin films have mosaic single crystal structure with (100) texture without regard to the Si substrate orientation. The investigations of PbTe/Si thin films dislocation density by the etching pits method and by the analysis of X-ray reflection profiles show the average values of about 10~5-10~7 cm~(-2). The experimental results of these methods have shown that PbTe/SiO_2/Si thin films had better crystallinity perfection. The average values of dislocation density were about 5X10~4-2X10~5 cm~(-2).
机译:改进的“热壁”技术(HWE)用于在具有和不具有任何缓冲层的Si(100)高欧姆衬底上直接生长PbTe薄膜。先前形成的SiO_2膜已经用作缓冲层。通过刻蚀坑法,SEM,RHEED以及X射线分析研究了PbTe薄膜的晶体微观结构,从而能够高精度地确定X射线摇摆曲线轮廓和线宽。这些PbTe / Si和PbTe / SiO_2 / Si薄膜具有具有(100)织构的镶嵌单晶结构,而与Si衬底的取向无关。通过刻蚀坑法和X射线反射谱分析研究了PbTe / Si薄膜的位错密度,结果表明其平均值约为10〜5-10〜7 cm〜(-2)。这些方法的实验结果表明,PbTe / SiO_2 / Si薄膜具有更好的结晶度。位错密度的平均值约为5X10〜4-2X10〜5 cm〜(-2)。

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