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Synthesis and Characterization of YAG:Ce Phosphor by Microwave Induced Combustion Synthesis with Different Fuel Sources

机译:Synthesis and Characterization of YAG:Ce Phosphor by Microwave Induced Combustion Synthesis with Different Fuel Sources

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White LEDs (WLEDs) have been produced from the combination of blue LED chips and phosphor converter. In the present work, considerable amount of yttrium aluminium garnet (YAG) phosphor powders doped with 0.3 mol% of cerium (Ce) have been synthesized via Microwave Induced Combustion Synthesis (MICS) method with different fuel sources such as urea and mixed fuel of urea and glycine. The effects of different fuel sources on the crystallinity, structure, luminescent properties and Commision International de L'Eclairage (CIE) chromaticity was characterized and studied using high resolution X-ray diffraction (HR XRD), field emission-scanning electron microscopy (FE SEM), energy dispersive X-ray spectroscopy (EDX), electroluminescence (EL) and standard CIE 1931 chromaticity diagram, respectively. The highest EL intensity can be observed from the sample prepared by mixed fuel technique. In contrast, the experimental enhancement in the aforementioned properties was demonstrated by the WLED synthesized using mixed fuel technique.
机译:白光LED(WLED)是由蓝光LED芯片和荧光粉转换器组合而成。本文采用微波诱导燃烧合成(MICS)方法,以尿素和尿素与甘氨酸的混合燃料为原料,合成了大量掺铈量为0.3mol%的钇铝石榴石(YAG)荧光粉。采用高分辨率X射线衍射(HR XRD)、场发射扫描电子显微镜(FE SEM)、能量色散X射线光谱仪(EDX)表征和研究了不同燃料源对结晶度、结构、发光性能和CIE色度的影响,分别为电致发光(EL)和标准CIE 1931色度图。通过混合燃料技术制备的样品可以观察到最高的EL强度。相比之下,使用混合燃料技术合成的WLED证明了上述性能的实验增强。

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