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Effects of preparation conditions on characters of hydrophobic silica granular aerogel and its Applications

机译:制备条件对疏水性二氧化硅粒状气凝胶特征及其应用的影响

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The hydrophobic silica granular aerogels were synthesized via sol-gel synthesis followed by ambient pressure drying. The tetraethyloxylane (TEOS) was used as original precursor. The aerogels were analyzed using nitrogen adsorption, scanning electron microscopy (SEM) and laser particle size analyzer. It was found that the aerogel was mesoporous material with high surface area. The aerogels were prepared in grain form by dipping into disperse solution in order to adsorption application. The average particle size of the aerogel was controlled by pH and disperse solution volume. The pH also affected gel time. The aerogels were used to absorb phenol from water. The saturated adsorption amount could reach up to 145 mg·g~(-1).
机译:通过溶胶 - 凝胶合成合成疏水性二氧化硅粒状气凝胶,然后通过环境压力干燥合成。四乙氧基(TEOS)用作原始前体。使用氮吸附,扫描电子显微镜(SEM)和激光粒度分析仪分析气凝胶。发现气凝胶是具有高表面积的中孔材料。通过浸入分散的溶液中以晶粒形式制备气凝胶以吸附施加溶液。通过pH和分散的溶液体积控制气凝胶的平均粒径。 pH也会影响凝胶时间。气凝胶用于吸收水中的苯酚。饱和吸附量可达145mg·g〜(-1)。

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