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Oxidation Behavior of Porous Ti_2AlC and Ti_3SiC_2 Produced by Powder Metallurgy

机译:粉末冶金生产多孔TI_2ALC和TI_3SIC_2的氧化行为

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The oxidation resistance of porous Ti_2AlC and Ti_3SiC_2 MAX phase compounds with controlled porosity and grain size obtained by powder metallurgy techniques was studied carrying out oxidation tests at different temperatures for each material depending on their maximum service temperature. The study was performed on isostatic consolidated samples with different percentage (20vol%, 60vol%) and size of space holder (250-400μm, 800-1000μm) and in samples without space holder. In order to understand the oxidation mechanism, oxidation kinetics were analyzed to determine the influence of size and amount of porosity in each case. In addition, the microstructure and composition of the oxide layers formed after the tests were analyzed by scanning electron microscopy (SEM).
机译:研究了具有受控孔隙率和通过粉末冶金技术获得的受控孔隙率和晶粒尺寸的多孔Ti_3SIC_2最大相化合物的抗氧化性,这取决于其最大的服务温度,在每个材料的不同温度下进行氧化试验。该研究对等静压固结样品进行,具有不同百分比(20Vol%,60Vol%)和空间支架(250-400μm,800-1000μm)和没有空间支架的样品的尺寸。为了理解氧化机理,分析氧化动力学以确定每种情况下孔隙率的尺寸和量的影响。另外,通过扫描电子显微镜(SEM)分析测试后形成的氧化物层的微观结构和组合物。

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