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FeCr_2O_4 SPINEL FORMATION: RELATIONSHIP BETWEEN COLOR AND MAGNETICS PROPERTIES

机译:FECR_2O_4尖晶石形成:颜色与磁性属性之间的关系

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Through reactions in solid form at high temperatures, using iron oxide (Fe_3O_4) and chromium oxide (Cr_2O_3) in fixed proportions as precursors, the compound was synthesized with spinel structure type FeCr_2O_4. For different temperatures synthesis was conducted the characterization of the material obtained through X-ray diffraction (XRD), spectroscopy UV-VIS-NIR, scanning electron microscopy (SEM), energy dispersion analysis of X-ray (EDX) thermal analysis (DTA / TGA) and magnetic susceptibility of alternating current. The changes in the spectra of reflectance changes are related to the phase identified, the degree of crystalline structure, the spatial order of cations and the magnetic behavior obtained.
机译:通过在高温下以固体形式的反应,在固定比例作为前体中使用氧化铁(Fe_3O_4)和氧化铬(Cr_2O_3),用尖晶石结构型FeCr_2O_4合成化合物。对于不同的温度合成,进行了通过X射线衍射(XRD),光谱uV-Vis-Nir,扫描电子显微镜(SEM),X射线(EDX)热分析的能量分散分析(DTA / TGA)和交流电流的磁化率。反射率变化光谱的变化与所识别的相位,结晶结构,阳离子的空间顺序和所获得的磁性行为有关。

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