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Preparation and performances of successive TiO2 thin film photocatalyst supported on carbon fiber

机译:碳纤维负载均负载的连续TiO2薄膜光催化剂的制备与性能

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Successive TiO2 film photocatalysts supported on surface modified PAN-carbon fiber (PAN-CF) substrates were prepared via the sol-gel dip-coating method with Ti(O4H9)4 as a precursor. Several techniques such as scanning electron microscope(SEM), thermogravimetric analysis (TGA), X-ray diffraction (XRD) were utilized to investigate the optimized concentrations of Ti sol, annealing temperature and their influence on the final properties of the TiO2/CF. The interfacial bonding properties of carbon fiber with TiO2 film was evaluated by ultrasonic vibration. The results show that M5TiO2/CF has favorable load fastness and load rate. The photocatalytic properties of TiO2/CF were investigated by degrading acid orange II (80mg/L) under UV irradiation. The results suggest that the catalytic activity have significant difference compared with M3TiO2/CF>M5TiO2/CF>M7TiO2/CF and the M5TiO2/CF has been shows the optimum catalytic performances.
机译:通过用Ti(O4H9)4作为前体,通过溶胶 - 凝胶浸涂方法制备表面改性泛碳纤维(PAN-CF)衬底上负载的连续TiO2薄膜光催化剂。使用诸如扫描电子显微镜(SEM),热重分析(TGA),X射线衍射(XRD)的几种技术,研究了Ti溶胶,退火温度及其对TiO 2 / CF最终性质的优化浓度。通过超声波振动评价碳纤维的碳纤维界面粘结性能。结果表明,M5TiO2 / CF具有良好的负载牢度和负载率。通过在紫外线照射下通过降解酸橙II(80mg / L)来研究TiO2 / CF的光催化性质。结果表明,与M3TiO2 / CF> M5TiO2 / CF> M7TiO 2 / CF相比,催化活性具有显着差异,并且M5TiO2 / CF已经显示出最佳的催化性能。

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