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The Role of Annealing Temperature Variation on ZnO Nanorods Array Deposited on TiO_2 Seed Layer

机译:退火温度变化对TiO_2种子层沉积ZnO纳米棒阵列的作用

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Seed layer of Titanium dioxide (TiO_2) by sol-gel spin coating technique were coated on glass substrate to grow Zinc oxide nanorods (ZNR) by solution-immersion method. The fabricated ZNR were annealed at various temperatures ranged from 400 to 600°C. FESEM images revealed that smaller ZNR were densely grown at optimum temperature of 450 and 500°C. Meanwhile, for all samples a dominant (0 0 2) diffraction peak of ZNR recorded by XRD patterns was at 34.4~0 which corresponding to hexagonal ZNR with a wurtzite structure. UV-Vis absorbance spectra showed the maximum absorption properties at UV region were detected at 450 and 500°C. The samples also showed high absorbance values at visible region.
机译:通过溶胶 - 凝胶旋转涂层技术涂覆二氧化钛(TiO_2)的种子层涂覆在玻璃基底上,通过溶液浸渍法生长氧化锌纳米棒(ZnR)。 在各种温度下退火制造的ZnR,范围为400至600℃。 FeSEM图像显示,较小的ZnR在最适温度为450和500℃的最佳温度下均匀地生长。 同时,对于所有样品,通过XRD图案记录的ZnR的显性(0 02)衍射峰值为34.4〜0,其对应于六边形ZnR,具有紫立岩结构。 UV-Vis吸光度光谱显示在450和500℃下检测UV区域的最大吸收性能。 样品还显示出可见区域的高吸光度值。

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