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AI2O3/Au Composite Coating on Stainless Steel Prepared by Electro-deposition

机译:电沉积法在不锈钢上制备Al2O3 / Au复合涂层

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Tritium permeation barriers on stainless steels are required in fusion technology in order to reduce the tritium permeation rate through the structural material into the cooling water system. Preparation of tritium permeation barrier AI2O3 is an important way to solve the problem of leakage of tritium permeation. It is worth to note that the noble Au is an excellent barrier of hydrogen dissolution. AI2O3/AU composite coating was designed for potential tritium permeation barrier on stainless steel. The alternation coatings have been prepared by electrochemical deposition method. The processing parameters and subsequent sinter temperature for composite coatings were optimized. The oxidation resistance of the coating has been tested. A hydrogen diffusion test simulating tritium permeation has been conducted to compare the sample with and without coating. Microstructure was examined by scanning electron microcopy (SEM). The results showed AI2O3/AU multi-alternation coatings can be prepared on the surface of stain less steel at the case of controlling processing well. The coatings have the characteristic of high temperature oxidation resistance and good hydrogen permeability barrier. The tritium permeation should be study further.
机译:在熔融技术中,需要在不锈钢上使用t渗透屏障,以降低通过结构材料进入冷却水系统的the渗透率。制备tri渗透阻挡层Al 2 O 3是解决tri渗透渗漏问题的重要途径。值得注意的是,高贵的金是氢溶解的极佳屏障。 AI2O3 / AU复合涂层被设计用于不锈钢上潜在的tri渗透阻挡层。交替涂层已经通过电化学沉积方法制备。优化了复合涂层的工艺参数和随后的烧结温度。涂层的抗氧化性已经过测试。已经进行了模拟tri渗透的氢扩散试验,以比较有涂层和无涂层的样品。通过扫描电子显微镜(SEM)检查微观结构。结果表明,在控制工艺条件下,可以在不锈钢表面制备Al2O3 / AU多涂层。该涂层具有耐高温氧化性和良好的氢渗透性阻挡层的特性。 t的渗透应进一步研究。

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