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Measuring temperature dependent viscosity of liquids using an atomic force microscope cantilever with a solid state heating element

机译:使用带有固态加热元件的原子力显微镜悬臂梁测量液体的温度相关粘度

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This paper presents a study on the dynamic response of an atomic force microscope (AFM) cantilever with a solid state heating element in liquid and its application for measuring the temperature-dependent viscosity of liquids. A finite difference model (FDM) predicts the frequency response of a heated cantilever immersed in liquid and calibrates the liquid viscosity from the measured cantilever resonant frequency (f) at different cantilever heater temperatures. The technique measures a wide range of liquid viscosities (0.0005-0.005 kgms) at temperatures ranging from 20 to 55 °C with high sensitivity (7.1 × 10 kgms/Hz for 50 wt% ethylene glycol/water). The measurement requires heating a liquid volume of about 10 nl, which is more than 1000X smaller than other microcantilever-based viscosity measurements.
机译:本文介绍了在液体中带有固态加热元件的原子力显微镜(AFM)悬臂的动态响应及其在测量液体的温度依赖性粘度中的应用。有限差分模型(FDM)可以预测浸入液体中的加热悬臂的频率响应,并根据在不同悬臂加热器温度下测得的悬臂共振频率(f)来校准液体粘度。该技术可在20至55°C的温度范围内以高灵敏度(对于50 wt%乙二醇/水为7.1×10 kgms / Hz)测量各种液体粘度(0.0005-0.005 kgms)。该测量需要加热约10 nl的液体体积,该液体体积比其他基于微悬臂梁的粘度测量结果小1000倍以上。

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