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Preparation and Photocatalytic Properties of Fe-Doped TiO2 Nanocrystalline Composite Particles

机译:掺铁TiO2纳米晶复合颗粒的制备及光催化性能

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Metatitanic acid was adopted as the raw material to prepare Fe-doped TiO2 nanocrystalline composite particles using suspension polymerization and sol-gel method,which were then characterized with XRD,TEM,TG-DTA and IR,etc..The results showed the samples were nanocrystal accumulated porous particles,with average particle size of 29nm.Through doping of Fe3+ ion,the photo catalytic activities of particles under Xe lamp were investigated by photodegrading the methyl orange.It was found that,the TiO2 nanocrystal doped with 0.5% Fe3+ ion (accounted as mass fraction) had the highest catalytic activity.The Fe-doped TiO2 nanocrystalline composite particles prepared in this study has high activity,is easy for separation,recovery and reuse.
机译:以偏钛酸为原料,采用悬浮聚合和溶胶-凝胶法制备了Fe掺杂的TiO2纳米晶复合颗粒,并通过XRD,TEM,TG-DTA和IR等对其进行了表征。纳米晶聚集了平均粒径为29nm的多孔颗粒。通过掺杂Fe3 +离子,对甲基橙进行光降解,研究了Xe灯下颗粒的光催化活性。发现TiO2纳米晶掺杂有0.5%Fe3 +离子(本研究制备的Fe掺杂的TiO2纳米晶复合颗粒具有较高的活性,易于分离,回收和再利用。

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