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MECHANICAL PROPERTIES AND CORROSION OF VACUUM SINTERED POWDER INJECTION MOLDED 316 L STAINLESS STEEL

机译:真空模压注射成型316 L不锈钢的力学性能和腐蚀

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Austenitic Stainless Steels (ASS) have vast applications in automotive, marine and medical due tohigh strength and corrosion resistance. This study presents the results of corrosion behavior of powderinjection molded 316L Stainless Steel parts. A spherical shape, water atomized 316L SS powder wasused in this study. Feedstock was prepared using Z-blade type mixer and viscosity was measuredusing a capillary rheometer. A vertical injection molding machine was used for injection molding oftest samples. The binder was removed by solvent extraction and thermal debinding followed bysintering in vacuum at 1325°C for 2 hrs. Heating and cooling rate of 5-10oC/min was maintained tominimize the evaporating species, Ni, Cr during the sintering process. Sintered test samples weretested for shrinkage, hardness and tensile strength. Corrosion response was of sintered test sampleswere measured by using weight loss method in Ringer’s Solution of PH 7.4 for 15 days. Sintereddensity achieved was approximately 96%. Tensile strength of test samples with 65 V% solid loadingwas 481MPa, elongation 22% and hardness 76HRB. The test samples sintered at 10oC/min andfollowed by the cooling at the same rate showed improved corrosion resistance compare to thosesintered at low heating and cooling rate. High cooling rate reduced the evaporation of Cr anddeveloped passive chromium oxide layer on the test samples during corrosion test and resultedreduced corrosion.
机译:由于以下原因,奥氏体不锈钢(ASS)在汽车,船舶和医疗领域具有广泛的应用 高强度和耐腐蚀性。这项研究提出了粉末腐蚀行为的结果 注塑316L不锈钢零件。球形水雾化316L SS粉末 在这项研究中使用。使用Z型叶片混合机制备原料并测量粘度 使用毛细管流变仪。立式注塑机用于注塑成型 测试样品。通过溶剂萃取和热脱脂,然后除去粘合剂来除去粘合剂 在真空中于1325°C烧结2小时。维持5-10oC / min的加热和冷却速度至 在烧结过程中尽量减少蒸发物质Ni,Cr。烧结测试样品是 测试收缩率,硬度和抗张强度。腐蚀响应是对烧结试样的 在林格氏pH 7.4溶液中使用减肥方法测量15天。烧结的 达到的密度约为96%。固含量为65 V%的试样的拉伸强度 为481MPa,伸长率为22%,硬度为76HRB。测试样品以10oC / min的速度烧结 然后以相同的速率冷却,与那些相比,具有更高的耐腐蚀性 在低加热和冷却速率下烧结。高冷却速率减少了Cr的蒸发 在腐蚀测试过程中在测试样品上形成钝化氧化铬层,结果 减少腐蚀。

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