Fictive Tg: Fact or Fiction? Part II

机译：虚构的Tg：事实还是虚构？第二部分

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A paper was submitted (Part 1) at the NATAS 2003 conference. At the end of the paper, an attendee strongly disagreed with both the conclusions and the data. Since there was insufficient time to respond to the comments, this paper will attempt to address the main issues. The attendee's basis for the strong disagreement included: 1. It is "Fictive Temperature" and not "Fictive Tg." 2. The temperature trend seen in the MDSC® Reversing signal on aged samples is an error caused by the use of only the first harmonic in the FT deconvolution process. 3. Tg can only be measured in cooling because of the superheating that can occur during heating.

机译：在NATAS 2003会议上提交了一篇论文（第1部分）。最后，与会者强烈不同意结论和数据。由于没有足够的时间来回应评论，因此本文将尝试解决主要问题。与会者之间存在强烈分歧的依据包括： 1.它是“虚构温度”，而不是“虚构Tg”。 2.在老化样品的MDSC®反转信号中看到的温度趋势是由于在FT反褶积过程中仅使用一次谐波而引起的误差。 3.由于在加热过程中可能发生过热，因此只能在冷却时测量Tg。

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《North American Thermal Analysis Society Annual Conference》|2004年|p.1-5|共5页
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Leonard C. Thomas; TA Instruments;
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