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Towards quality excellence in radioanalytical laboratories at STUK, Finland

机译:致力于芬兰STUK放射分析实验室的卓越质量

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摘要

The development of a uniform and modern quality system for the whole of the Finnish Radiation and Nuclear Safety Authority (STUK) began in 1997. The principle of continuous improvement is widely applied by performing annual self-assessments as well as internal and external audits. One of the most important steps in a quality assurance programme is the proficiency of the personnel. Good initiation, non-stop training during work and knowledge of the physical and chemical properties that affect analytical procedures are the requirements for first-rate and motivated working. Working procedures have been planned and followed through in order to prevent any contamination in laboratories. Considerable emphasis has also been placed on the standardisation of uncertainty estimations. This demands good knowledge of the sources of errors in sample preparation, analysis and measurement. Participating in intercomparison exercises and proficiency tests is one way to demonstrate the validity and quality of the methods used. However, a lack of intercomparison exercises and reference material on certain natural radionuclides occurring in waters and certain artificial radionuclides has complicated the validation and proficiency testing of these measurements. Moreover, the arrangement of intercomparisons has not always been optimal.
机译:1997年开始为整个芬兰辐射和核安全局(STUK)建立统一和现代化的质量体系。通过进行年度自我评估以及内部和外部审核,持续改进的原则得到了广泛应用。质量保证计划中最重要的步骤之一就是人员的熟练程度。一流而有动力的工作要求,要有良好的启动,工作期间不间断的培训以及对影响分析程序的物理和化学性质的了解。为了防止实验室受到污染,已经计划并遵循了工作程序。不确定性估计的标准化也得到了相当大的重视。这要求对样品制备,分析和测量中的错误来源有充分的了解。参加比对练习和能力测试是证明所用方法的有效性和质量的一种方法。但是,由于缺乏对水中某些天然放射性核素和某些人工放射性核素的比对练习和参考资料,使这些测量的验证和能力测试变得复杂。此外,比对的安排并不总是最佳的。

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