AbstractSyndiotactic polystyrene and copolymers of styrene and p‐methylstyrene were synthetized in bulk by using a titanium tetraethoxide/methylaluminoxane catalytic system. The polymers were analyzed by13C and1H Nuclear Magnetic Resonance, Infrared Spectroscopy, Gel Permeation Chromatography and Differential Scanning Calorimetry and their properties were compare
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